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Phys. Rev. Lett. 100, 206101 (2008) [4 pages]

Quantitative Atomic Resolution Scanning Transmission Electron Microscopy

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James M. LeBeau1,*, Scott D. Findlay2, Leslie J. Allen3, and Susanne Stemmer4,†
1Materials Department, University of California, Santa Barbara, California 93106-5050, USA
2Institute of Engineering Innovation, School of Engineering, The University of Tokyo, Tokyo, 113-8656, Japan
3School of Physics, University of Melbourne, Victoria 3010, Australia
4Materials Department, University of California, Santa Barbara, California 93106-5050, USA

Received 1 February 2008; revised 16 April 2008; published 23 May 2008

Complete understanding of atomic resolution high-angle annular dark-field (Z-contrast) images requires quantitative agreement between simulations and experiments. We show that intensity variations can be placed on an absolute scale by normalizing the measured image intensities to the incident beam. We construct fractional intensity images of a SrTiO3 single crystal for regions of different thickness up to 120 nm. Experimental images are compared directly with image simulations. Provided that spatial incoherence is taken into account in the simulations, almost perfect agreement is found between simulation and experiment.

© 2008 The American Physical Society

URL:
http://link.aps.org/doi/10.1103/PhysRevLett.100.206101
DOI:
10.1103/PhysRevLett.100.206101
PACS:
68.37.Lp

*lebeau@mrl.ucsb.edu

stemmer@mrl.ucsb.edu