Electrical impedance spectroscopy of microchannel-nanochannel interface devices

Accepted

We report experimental verification of the depression of the slope in the Warburg branch of the electrochemical impedance spectrum using a fabricated microchannel-nanochannel device. This was previously theoretically predicted to occur with increasing DC bias voltage as a result of nanochannel EOF, and provides an example of the influence of net fluid flow on electrokinetic transport. The dominant influence of nanochannel polarization in the kHz-range of the impedance response is also demonstrated experimentally. This latter effect may be significant in both fundamental electrokinetics of micro-nanochannel devices as well as in practical molecular sensing applications.